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21,58 61 A representative uorescence spectrum (along with an excitation line at 340 nm) from a single microreactor in the array is illustrated in Figure 53B The rst-order measurements were used for the optimization of melt-polymerization reaction conditions as described in Section 51 When measurements are done with a rst-order instrument, and there is another independent variable involved, this constitutes a second-order measurement approach This type of screening was used for the in situ monitoring of melt-polymerization reactions (see Section 54) and for the evaluation of the sensor materials Figure 54A shows a 48-element array of sensor materials positioned in a gas ow-cell for the monitoring of the materials response upon exposure to vapors of interest For the evaluation of sensor materials, absorption spectra were collected over a period of time of reaction of these sensor materials with a vapor of interest.

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Results of these measurements are illustrated in Figure 54B Adding two more independent variable parameters to the response of a rst-order system obviously makes it a third-order measurement approach An example of such system is spectroscopic monitoring (wavelength is the variable parameter I) of the reaction progress of combinatorial materials (time is the variable parameter J) at different process temperatures (temperature is the variable parameter K) Alternatively, a second-order system can be implemented for the measurements as a function of one or more independent parameters Examples of second-order systems are excitationemission luminescence measurement systems, GC-MS, and HPLC-diode array UV systems, among others An example of one of our third-order measurement approaches for combinatorial screening is illustrated in Figure 55 It was implemented for the determination of oxidative stability of polymers under different process conditions (temperature I and time J).

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